The stable organic solution of dichloroglyoxime was prepared in high yield by chlorine aerated into the ethylene glycol solution of glyoxime.

将乙二肟溶于乙二醇,通入氯气,生成稳定的二氯乙二肟溶液,这种方法制备的二氯乙二肟贮存稳定,产率高。